2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

Base Information

Chemical Name:2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide
CAS No.:219921-88-7
Molecular Formula:C₁₅H₁₉ClN₂
Molecular Weight:262.782
Hs Code.:

Synonyms:2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

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Chemical Property of 2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

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Technology Process of 2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

There total 1 articles about 2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219921-87-6
5-chloro-2-piperidino-benzylcyanide

: 74-88-4
methyl iodide

: 219921-88-7
2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) DMF, from 40 deg C to 50 deg C, 0.5 h, 2.) DMF, RT, 2 h;
DOI:10.1021/jm9810349

Reference yield: 68.0%

: 219921-88-7
2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

: 2-(5-chloro-2-piperidino-phenyl)-2-methyl-propanoyl-amine

Guidance literature:: With sulfuric acid; at 50 ℃; for 3h;
DOI:10.1021/jm9810349

Reference yield:

: 219921-88-7
2-(5-chloro-2-piperidino-phenyl)-2-propylcyanide

: N,N'-bis-(2-(5-chloro-2-piperidino-phenyl)-2-propyl)-urea

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 85 percent aq. H₂SO₄ / 3 h / 50 °C

2: aq. NaOBr / dioxane / 0 - 20 °C

With sodium hypobromide; sulfuric acid; In 1,4-dioxane;
DOI:10.1021/jm9810349