ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

Base Information

Chemical Name:ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate
CAS No.:121045-64-5
Molecular Formula:C₂₂H₁₉NO₃
Molecular Weight:345.398
Hs Code.:

ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benz<f>indole-2-carboxylate

Synonyms:ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

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Chemical Property of ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

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Technology Process of ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

There total 2 articles about ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121045-62-3
2-<(1-benzyl-5-ethoxycarbonylpyrrol-3-yl)methyl>benzoic acid

: 121045-64-5
ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

Guidance literature:: With trifluoroacetic anhydride; In trifluoroacetic acid; for 1h; Ambient temperature;

Reference yield:

: 121045-63-4
ethyl 1-benzyl-4-(2-benzyloxycarbonylbenzyl)pyrrole-2-carboxylate

: 121045-64-5
ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / hydrogen / 10percent Pd/C / ethanol / 45 h / Ambient temperature

2: 80 percent / TFAA / trifluoroacetic acid / 1 h / Ambient temperature

With hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethanol; trifluoroacetic acid;

Reference yield: 96.0%

: 121045-64-5
ethyl 1-benzyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

: 121045-65-6
ethyl 1-benzyl-4,9-dioxo-4,9-dihydro-1H-benzindole-2-carboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; N,N-dimethyl-formamide; for 48h; Ambient temperature; in DMSO without DDQ, RT, 24 h;