((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

Base Information

Chemical Name:((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine
CAS No.:107982-90-1
Molecular Formula:C₆H₇N*C₁₇H₂₆N₂O₈S
Molecular Weight:511.596
Hs Code.:

Synonyms:((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

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Chemical Property of ((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

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Technology Process of ((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

There total 5 articles about ((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2280-28-6,5174-30-1
3-hydroxy-DL-valine

: 107982-90-1
((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 2-methyl-propan-2-ol; H₂O / pH= 10

2: DCC, HOBT / ethyl acetate

3: various solvent(s) / 2 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In water; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)84643-2

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 107982-90-1
((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 2-methyl-propan-2-ol; H₂O / pH= 10

2: DCC, HOBT / ethyl acetate

3: various solvent(s) / 2 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In water; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)84643-2

Reference yield:

: 102507-13-1,105504-72-1
N-(tert-butoxycarbonyl)-3-hydroxy-L-valine

: 107982-90-1
((S)-1-Benzyloxycarbamoyl-2-methyl-2-sulfooxy-propyl)-carbamic acid tert-butyl ester; compound with 2-methyl-pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: DCC, HOBT / ethyl acetate

2: various solvent(s) / 2 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1016/S0040-4039(00)84643-2