1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide

Base Information

• Chemical Name: 1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide
• CAS No.: 261900-45-2
• Molecular Formula: C₁₄H₁₁ClN₂O₃S
• Molecular Weight: 322.772

Synonyms:1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide

Chemical Property of 1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide

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Technology Process of 1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide

There total 1 articles about 1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide (2225-37-8) + 1-Chloro-3-chloromethyl-benzene (620-20-2,130468-19-8) → 1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide (261900-45-2)

Guidance literature:

With sodium hydrogencarbonate; for 2h; Heating;

DOI:10.1021/jm990382n

Reference yield: 44.0%

benzyl bromide (100-39-0) + 1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide (261900-45-2) → 3-benzyl-1-(3-chloro-benzyl)-2,2-dioxo-2,3-dihydro-1H-2λ6-benzo[1,2,6]thiadiazin-4-one + 4-benzyloxy-1-(3-chloro-benzyl)-1H-benzo[1,2,6]thiadiazine 2,2-dioxide

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 2h; Heating;

DOI:10.1021/jm000118q

Reference yield:

1-[(3-chlorophenyl)methyl]-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide (261900-45-2) → 3-benzyl-1-(3-chloro-benzyl)-2,2-dioxo-2,3-dihydro-1H-2λ6-benzo[1,2,6]thiadiazin-4-one

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; Heating;

DOI:10.1016/S0960-894X(99)00538-7

upstream raw materials:

1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide

1-Chloro-3-chloromethyl-benzene

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