7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on

Base Information

• Chemical Name: 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on
• CAS No.: 75848-06-5
• Molecular Formula: C₃₀H₂₇N₃O₁₂
• Molecular Weight: 621.557

Synonyms:7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on

Chemical Property of 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on

There total 3 articles about 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-7,8-dihydro-1,3-dioxolo<4,5-g>isochinolinium-perchlorat → 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on (75848-06-5)

Guidance literature:

With potassium permanganate; ammonia; In acetic acid; acetone; for 20h; Ambient temperature;

DOI:10.1002/ardp.19803130811

Reference yield:

4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-ol (82-54-2) → 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on (75848-06-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 40 percent / ethanol / 0.67 h / Heating

2: 80 percent / 70percent aq. HClO₄ / 16 h / Heating

3: 75 percent / ammonia, KMnO₄ / acetone; aq. acetic acid / 20 h / Ambient temperature

With potassium permanganate; perchloric acid; ammonia; In ethanol; acetic acid; acetone;

DOI:10.1002/ardp.19803130811

Reference yield:

8-(α-Hydroxy-2-nitrobenzyl)-4-methoxy-6-methyl-10-(2-nitrophenyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin (75836-98-5) → 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on (75848-06-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 70percent aq. HClO₄ / 16 h / Heating

2: 75 percent / ammonia, KMnO₄ / acetone; aq. acetic acid / 20 h / Ambient temperature

With potassium permanganate; perchloric acid; ammonia; In acetic acid; acetone;

DOI:10.1002/ardp.19803130811

upstream raw materials:

4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-ol

8-(α-Hydroxy-2-nitrobenzyl)-4-methoxy-6-methyl-10-(2-nitrophenyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 75848-06-5 7,8-Bis(α-acetoxy-2-nitrobenzyl)-4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo<4,5-g>isochinolin-5-on

Send

Send

Metric Ton KG G Pound L ML

Send

Send