4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Base Information

Chemical Name:4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical
CAS No.:886546-74-3
Molecular Formula:C₂₂H₂₄NO₃
Molecular Weight:350.437
Hs Code.:

Synonyms:4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

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Chemical Property of 4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

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Technology Process of 4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

There total 1 articles about 4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: (4-benzoylphenyl)boronic acid

: 85591-93-1
3-bromo-4-hydroxymethyl-2,2,5,5-tetramethyl-Δ³-pyrrolin-1-oxyl

: 886546-74-3
4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: With aq. NaCO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 4h; Heating;
DOI:10.1055/s-2006-926279

Reference yield:

: 886546-74-3
4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

: 124-63-0
methanesulfonyl chloride

: C₂₃H₂₆NO₅S

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1055/s-2006-926279

Reference yield:

: 886546-74-3
4-(4-benzoylphenyl)-3-hydroxymethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

: 886546-77-6
4-(4-benzoylphenyl)-3-bromomethyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1 h / 20 °C

2: 404 mg / LiBr / acetone / 0.5 h / Heating

With triethylamine; lithium bromide; In dichloromethane; acetone;
DOI:10.1055/s-2006-926279