phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Base Information

Chemical Name:phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate
CAS No.:261895-32-3
Molecular Formula:C₂₆H₂₆N₂O₂
Molecular Weight:398.505
Hs Code.:

Synonyms:phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

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Technology Process of phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

There total 3 articles about phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₂₆H₂₈N₂O₂

: 261895-32-3
phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Guidance literature:: With copper(I) trifluoromethanesolfonate toluene complex; In dichloromethane; acetonitrile; at 20 ℃; for 2h;
DOI:10.1002/ejoc.201600246

Reference yield: 50.0%

: 261895-24-3
phenylmethyl 3-ethylidene-4-[(1-methylindol-2-yl)ethylidene]piperidine-1-carboxylate

: 261895-32-3
phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Guidance literature:: In benzene; for 3h; Irradiation;
DOI:10.1016/S0040-4020(99)01016-9

Reference yield:

: 603-76-9
1-methylindole

: 261895-32-3
phenylmethyl 5,6,11-trimethyl-1,2,3,4-tetrahydropyrido[4,3-b]carbazole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuLi, 2.) BEt₃, 3.) PdCl₂(PPh₃)2 / 1.) THF, 2.) THF, 60 deg C, 30 min

2: 50 percent / benzene / 0 °C / Irradiation

With bis-triphenylphosphine-palladium(II) chloride; triethyl borane; tert.-butyl lithium; In benzene;
DOI:10.1055/s-1997-746