Technology Process of MRT-14
There total 7 articles about MRT-14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) chloride; sodium hydroxide;
In
acetonitrile;
at 120 ℃;
for 0.1h;
under 2585.81 Torr;
Inert atmosphere;
Microwave irradiation;
DOI:10.1021/jm2013369
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; ammonium formate / isopropyl alcohol / Inert atmosphere; Microwave irradiation
2: acetone / 1 h / Inert atmosphere; Reflux
3: copper(l) chloride; sodium hydroxide / acetonitrile / 0.1 h / 120 °C / 2585.81 Torr / Inert atmosphere; Microwave irradiation
With
palladium 10% on activated carbon; ammonium formate; copper(l) chloride; sodium hydroxide;
In
isopropyl alcohol; acetone; acetonitrile;
DOI:10.1021/jm2013369
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetone / 1 h / Inert atmosphere; Reflux
2: copper(l) chloride; sodium hydroxide / acetonitrile / 0.1 h / 120 °C / 2585.81 Torr / Inert atmosphere; Microwave irradiation
With
copper(l) chloride; sodium hydroxide;
In
acetone; acetonitrile;
DOI:10.1021/jm2013369