5-Phenoxy-pentanedithioic acid methyl ester

Base Information

Chemical Name:5-Phenoxy-pentanedithioic acid methyl ester
CAS No.:192226-23-6
Molecular Formula:C₁₂H₁₆OS₂
Molecular Weight:240.39
Hs Code.:

Synonyms:5-Phenoxy-pentanedithioic acid methyl ester

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Chemical Property of 5-Phenoxy-pentanedithioic acid methyl ester

Chemical Property:

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Technology Process of 5-Phenoxy-pentanedithioic acid methyl ester

There total 1 articles about 5-Phenoxy-pentanedithioic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 74-88-4
methyl iodide

: 192226-23-6
5-Phenoxy-pentanedithioic acid methyl ester

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1039/a701942d

Reference yield: 98.0%

: 192226-23-6
5-Phenoxy-pentanedithioic acid methyl ester

: 74-88-4
methyl iodide

: 192226-25-8
(5,5-Bis-methylsulfanyl-pent-4-enyloxy)-benzene

Guidance literature:: With lithium diisopropyl amide;
DOI:10.1039/a701942d

Reference yield:

: 192226-23-6
5-Phenoxy-pentanedithioic acid methyl ester

: (Z)-1-Methylsulfanyl-5-phenoxy-pent-1-en-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / LDA

2: 60 percent / MCPBA

3: PhSNa / methanol / 96 h / Ambient temperature

With sodium thiophenolate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In methanol;
DOI:10.1039/a701942d