tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

Base Information

Chemical Name:tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate
CAS No.:1643461-48-6
Molecular Formula:C₂₅H₄₁NO₄
Molecular Weight:419.605
Hs Code.:

Synonyms:tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

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Chemical Property of tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

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Technology Process of tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

There total 1 articles about tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1806-26-4
p-Octylphenol

: 196964-41-7
rac-tert-butyl 2,2-dimethyl-4-[(tosyloxy)methyl]-oxazolidine-3-carboxylate

: 1643461-48-6
tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

Guidance literature:: p-Octylphenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h;

rac-tert-butyl 2,2-dimethyl-4-[(tosyloxy)methyl]-oxazolidine-3-carboxylate; In N,N-dimethyl-formamide; mineral oil; at 70 ℃; for 3h;
DOI:10.1039/c4ob00535j

Reference yield: 99.0%

: 1643461-48-6
tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

: 2-amino-3-(4-octylphenoxy)propan-1-ol hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; diethyl ether; at 20 ℃; for 12h;
DOI:10.1039/c4ob00535j

Reference yield:

: 1643461-48-6
tert-butyl 2,2-dimethyl-4-[(4-octylphenoxy)methyl]oxazolidine-3-carboxylate

: 1643461-49-7
tert-butyl [1-hydroxy-3-(4-octylphenoxy)propan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; diethyl ether / 12 h / 20 °C

2: triethylamine / methanol; diethyl ether / 12 h / 0 °C

With hydrogenchloride; triethylamine; In methanol; diethyl ether;
DOI:10.1039/c4ob00535j