(1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

Base Information

Chemical Name:(1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride
CAS No.:138560-22-2
Molecular Formula:C₈H₁₇NO₅*ClH
Molecular Weight:243.688
Hs Code.:

Synonyms:(1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

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Chemical Property of (1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

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Technology Process of (1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

There total 4 articles about (1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 138560-21-1
(-)-(3aα,4β,5α,6β,7α,7aα)-octahydro-1-methyl-4,5,6,7-tetrakis(phenylmethoxy)-2,1-benzisoxazole

: 138560-22-2
(1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

Guidance literature:: With hydrogen; palladium; In acetic acid; for 48h;
DOI:10.1016/S0040-4020(01)88278-8

Reference yield:

: 73111-58-7,130861-06-2,73111-15-6
2,3,4-tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose

: 138560-22-2
(1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

2: 40 percent / N-chlorosuccinimde (NCS), AgNO₃ / acetonitrile; H₂O / 0.75 h

3: 60 percent / methanol / 1.) reflux, 4 h, 2.) 25 deg C, 2.5 d

4: 76 percent / H₂ / Pd black / acetic acid / 48 h

With N-chloro-succinimide; hydrogen; silver nitrate; palladium; In methanol; water; acetic acid; acetonitrile;
DOI:10.1016/S0040-4020(01)88278-8

Reference yield:

: 138560-18-6,138560-30-2
6,7-dideoxy-2,3,4,5-tetrakis-O-(phenylmethyl)-D-gulo/ido-hept-6-enose, cyclic 1,3-propanediyl mercaptals

: 138560-22-2
(1R,2S,3S,4R,5S,6S)-5-(hydroxymethyl)-6-(methylamino)cyclohexane-1,2,3,4-tetraol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / N-chlorosuccinimde (NCS), AgNO₃ / acetonitrile; H₂O / 0.75 h

2: 60 percent / methanol / 1.) reflux, 4 h, 2.) 25 deg C, 2.5 d

3: 76 percent / H₂ / Pd black / acetic acid / 48 h

With N-chloro-succinimide; hydrogen; silver nitrate; palladium; In methanol; water; acetic acid; acetonitrile;
DOI:10.1016/S0040-4020(01)88278-8