C₂₄H₃₅N₇O₉S

Base Information

Chemical Name:C₂₄H₃₅N₇O₉S
CAS No.:221448-89-1
Molecular Formula:C₂₄H₃₅N₇O₉S
Molecular Weight:597.649
Hs Code.:

C<sub>24</sub>H<sub>35</sub>N<sub>7</sub>O<sub>9</sub>S

Synonyms:C₂₄H₃₅N₇O₉S

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Chemical Property of C₂₄H₃₅N₇O₉S

Chemical Property:

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Technology Process of C₂₄H₃₅N₇O₉S

There total 9 articles about C₂₄H₃₅N₇O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21568-87-6
2-aminocaprolactam

: 221448-89-1
C₂₄H₃₅N₇O₉S

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / aq. NaHCO₃ / tetrahydrofuran / 0 - 20 °C

2: 91 percent / LiN(TMS)2 / tetrahydrofuran / 0 - 20 °C

3: 99 percent / HCl / ethyl acetate / 0 - 20 °C

4: 87 percent / Et₃N / acetonitrile / 0 - 20 °C

5: 100 percent / H₂ / Pd/C / methanol / 2327.2 Torr

6: 66 percent / EDC, HOBt, DIEA / acetonitrile / Ambient temperature

7: 1.) aq. LiOH, 2.) HOAc / 1.) EtOH, RT, 3 d

With hydrogenchloride; lithium hydroxide; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate; acetonitrile;
DOI:10.1016/S0960-894X(98)00667-2

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 221448-89-1
C₂₄H₃₅N₇O₉S

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Cl₂, 2.) thiourea, 3.) aq. Cl₂

2: 87 percent / Et₃N / acetonitrile / 0 - 20 °C

3: 100 percent / H₂ / Pd/C / methanol / 2327.2 Torr

4: 66 percent / EDC, HOBt, DIEA / acetonitrile / Ambient temperature

5: 1.) aq. LiOH, 2.) HOAc / 1.) EtOH, RT, 3 d

With lithium hydroxide; hydrogen; chlorine; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; thiourea; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/S0960-894X(98)00667-2

Reference yield:

: 76944-95-1
tert-butyl N-[(3S)-2-oxoazepan-3-yl]carbamate

: 221448-89-1
C₂₄H₃₅N₇O₉S

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / LiN(TMS)2 / tetrahydrofuran / 0 - 20 °C

2: 99 percent / HCl / ethyl acetate / 0 - 20 °C

3: 87 percent / Et₃N / acetonitrile / 0 - 20 °C

4: 100 percent / H₂ / Pd/C / methanol / 2327.2 Torr

5: 66 percent / EDC, HOBt, DIEA / acetonitrile / Ambient temperature

6: 1.) aq. LiOH, 2.) HOAc / 1.) EtOH, RT, 3 d

With hydrogenchloride; lithium hydroxide; hydrogen; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate; acetonitrile;
DOI:10.1016/S0960-894X(98)00667-2