cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

Base Information

Chemical Name:cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine
CAS No.:1397712-46-7
Molecular Formula:C₁₈H₂₆N₂O₄S
Molecular Weight:366.481
Hs Code.:

Synonyms:cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

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Chemical Property of cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

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Technology Process of cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

There total 8 articles about cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1397712-45-6
3-(2-cyclohexylamino-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-5-yl)phenol

: 74-88-4
methyl iodide

: 1397712-46-7
cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

Guidance literature:: With 1-methyl-pyrrolidin-2-one; potassium tert-butylate; at 20 ℃;

Reference yield:

: 1397712-42-3
[5-(3-benzyloxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]cyclohexylamine

: 1397712-46-7
cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 51.5 h / Inert atmosphere

2: potassium tert-butylate; 1-methyl-pyrrolidin-2-one / 20 °C

With 1-methyl-pyrrolidin-2-one; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; In methanol;

Reference yield:

: 191097-27-5
methanesulfonic acid 3-benzyloxybenzyl ester

: 1397712-46-7
cyclohexyl-[5-(3-methoxyphenyl)-6,6-dimethyl-4,4-dioxo-5,6-dihydro-4H-4lambda6-[1,4,3]-oxathiazin-2-yl]amine

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium sulfite / water / 5 h / 90 °C

2.1: oxalyl dichloride / tetrahydrofuran; N,N-dimethyl-formamide; diethyl ether / 0.25 h / -20 - 0 °C / Inert atmosphere

3.1: tetrahydrofuran; ethyl acetate / 0.5 h / -20 - 0 °C / Inert atmosphere

4.1: phenyllithium / tetrahydrofuran / -75 - 0 °C / Inert atmosphere

4.2: 0.17 h / -75 °C / Cooling

4.3: 2.5 h / 20 °C

5.1: 1-methyl-pyrrolidin-2-one; sodium hexamethyldisilazane / tetrahydrofuran / 1.08 h / 20 °C

5.2: 1 h / 20 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol / 51.5 h / Inert atmosphere

7.1: potassium tert-butylate; 1-methyl-pyrrolidin-2-one / 20 °C

With 1-methyl-pyrrolidin-2-one; oxalyl dichloride; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; sodium hexamethyldisilazane; phenyllithium; sodium sulfite; In tetrahydrofuran; methanol; diethyl ether; water; ethyl acetate; N,N-dimethyl-formamide;