2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

Base Information

Chemical Name:2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide
CAS No.:1027541-38-3
Molecular Formula:C₂₁H₂₀N₂O₄S
Molecular Weight:396.467
Hs Code.:

Synonyms:2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

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Chemical Property of 2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

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Technology Process of 2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

There total 3 articles about 2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026811-44-8
3-Benzylsulfanyl-2-methoxy-N-(4-methoxy-phenyl)-isonicotinamide

: 1027541-38-3
2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/jm00045a012

Reference yield:

: 150-60-7
dibenzyl disulphide

: 1027541-38-3
2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, a. -78 deg C, 30 min, b. -23 deg C, 45 min, 2.) THF, from -78 deg C to 25 deg C, 1 h

2: 3-chloroperbenzoic acid / CH₂Cl₂ / 0.25 h / 0 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00045a012

Reference yield:

: 2-Methoxy-N-(4-methoxy-phenyl)-isonicotinamide

: 1027541-38-3
2-Methoxy-N-(4-methoxy-phenyl)-3-phenylmethanesulfinyl-isonicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, a. -78 deg C, 30 min, b. -23 deg C, 45 min, 2.) THF, from -78 deg C to 25 deg C, 1 h

2: 3-chloroperbenzoic acid / CH₂Cl₂ / 0.25 h / 0 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00045a012