2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Base Information

Chemical Name:2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate
CAS No.:79289-85-3
Molecular Formula:C₂₈H₃₆O₁₁S₂
Molecular Weight:612.719
Hs Code.:

Synonyms:2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Suppliers and Price of 2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

There total 3 articles about 2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 79289-86-4
2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol

: 98-59-9
p-toluenesulfonyl chloride

: 79289-85-3
2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Guidance literature:: In pyridine; at 0 ℃; for 12h;
DOI:10.1021/ja00410a041

Reference yield:

: 14496-24-3
3,4-bis(hydroxymethyl)furan

: 79289-85-3
2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaH / dimethylformamide / 48 h / Ambient temperature

2: 97 percent / Dowex 50W-X₁₂ / methanol; CH₂Cl₂ / 12 h / Heating

3: 84 percent / pyridine / 12 h / 0 °C

With Dowex 50W-X₁₂; sodium hydride; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00410a041

Reference yield:

: 79289-84-2
2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))bis-(tetrahydro-2H-pyran)

: 79289-85-3
2,2'-(3,4-furandiylbis(methyleneoxyethyleneoxy))-diethanol di-p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / Dowex 50W-X₁₂ / methanol; CH₂Cl₂ / 12 h / Heating

2: 84 percent / pyridine / 12 h / 0 °C

With Dowex 50W-X₁₂; In pyridine; methanol; dichloromethane;
DOI:10.1021/ja00410a041