O-Benzyl-2-bromo-N-methylacetohydroxamic acid

Base Information

• Chemical Name: O-Benzyl-2-bromo-N-methylacetohydroxamic acid
• CAS No.: 224557-85-1
• Molecular Formula: C₁₀H₁₂BrNO₂
• Molecular Weight: 258.115

Synonyms:O-Benzyl-2-bromo-N-methylacetohydroxamic acid

Chemical Property of O-Benzyl-2-bromo-N-methylacetohydroxamic acid

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

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Technology Process of O-Benzyl-2-bromo-N-methylacetohydroxamic acid

There total 1 articles about O-Benzyl-2-bromo-N-methylacetohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

O-benzyl-N-methylhydroxylamine hydrochloride (71925-14-9) + 2-Bromoacetyl bromide (598-21-0) → O-Benzyl-2-bromo-N-methylacetohydroxamic acid (224557-85-1)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; for 7h; Ambient temperature;

DOI:10.1039/DT9950002565

Reference yield: 87.0%

1,4,8,11-Tetraazacyclotetradecane (295-37-4) + O-Benzyl-2-bromo-N-methylacetohydroxamic acid (224557-85-1) → 1,4,8,11-tetraazacyclotetradecane-N,N',N-tris(O-benzyl-N-methylacetohydroxamic acid)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 18h;

DOI:10.1002/cplu.201600003

Reference yield: 82.0%

1,5,9-triazacyclododecane (294-80-4) + O-Benzyl-2-bromo-N-methylacetohydroxamic acid (224557-85-1) → 1,5,9-Triazacyclododecane-N,N',N''-tris(O-benzyl-N-methylacetohydroxamic acid)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; 1.) 90-100 deg C, 2 h, 2.) r.t., 18 h;

DOI:10.1039/DT9950002565

upstream raw materials:

O-benzyl-N-methylhydroxylamine hydrochloride

2-Bromoacetyl bromide

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