tert-butyl N-(2,4-dinitrophenoxy)carbamate

Base Information

Chemical Name:tert-butyl N-(2,4-dinitrophenoxy)carbamate
CAS No.:17508-16-6
Molecular Formula:C11H13 N3 O7
Molecular Weight:299.24
Hs Code.:2924299090
NSC Number:131108,208403
DSSTox Substance ID:DTXSID30938620
Nikkaji Number:J3.400.572I
Mol file:17508-16-6.mol

Synonyms:17508-16-6;tert-butyl N-(2,4-dinitrophenoxy)carbamate;TERT-BUTYL (2,4-DINITROPHENOXY)CARBAMATE;tert-butyl 2,4-dinitrophenoxycarbamate;NSC131108;SCHEMBL7647976;DTXSID30938620;t-butyl 2,4-dinitrophenoxycarbamate;NSC208403;AKOS024341803;NSC-131108;NSC-208403;tert-Butyl hydrogen (2,4-dinitrophenoxy)carbonimidate

Suppliers and Price of tert-butyl N-(2,4-dinitrophenoxy)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of tert-butyl N-(2,4-dinitrophenoxy)carbamate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：139.20000
Density:1.388g/cm³
LogP:3.75880
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:299.07534976
Heavy Atom Count:21
Complexity:410

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NOC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of tert-butyl N-(2,4-dinitrophenoxy)carbamate

There total 4 articles about tert-butyl N-(2,4-dinitrophenoxy)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 17508-16-6
tert-butyl (2,4-dinitrophenoxy)carbamate

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; at 0 - 5 ℃; for 2h;
DOI:10.1021/acs.orglett.5b00392

Reference yield:

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 17508-16-6
tert-butyl (2,4-dinitrophenoxy)carbamate

Guidance literature:: With potassium hydroxide;
DOI:10.1016/S0040-4020(01)93831-1

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 17508-16-6
tert-butyl (2,4-dinitrophenoxy)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; hydroxylamine hydrochloride / tetrahydrofuran; water

2: potassium hydroxide / tetrahydrofuran / 2 h / 0 - 5 °C

With hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1021/acs.orglett.5b00392