(E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

Base Information

Chemical Name:(E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone
CAS No.:1026295-20-4
Molecular Formula:C₂₈H₃₆O₁₀
Molecular Weight:532.588
Hs Code.:

Synonyms:(E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

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Chemical Property of (E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

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Technology Process of (E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

There total 5 articles about (E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 65490-09-7
2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone

: 495412-07-2
3,4-bis(methoxymethoxy)-2-(3-methylbut-2-enyl)benzaldehyde

: 1026295-20-4
(E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

Guidance literature:: With potassium hydroxide; In ethanol; water; for 36h; Ambient temperature;
DOI:10.1080/00304949609356517

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 1026295-20-4
(E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / K₂CO₃ / acetone / 0.5 h / Heating

2: 88 percent / KOH / ethanol; H₂O / 36 h / Ambient temperature

With potassium hydroxide; potassium carbonate; In ethanol; water; acetone;
DOI:10.1080/00304949609356517

Reference yield:

: 870-63-3
prenyl bromide

: 1026295-20-4
(E)-3-[3,4-Bis-methoxymethoxy-2-(3-methyl-but-2-enyl)-phenyl]-1-(2-hydroxy-4,6-bis-methoxymethoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: 24 percent / KOH / H₂O / 24 h / Ambient temperature

2: 85 percent / K₂CO₃ / acetone / 0.5 h / Heating

3: 88 percent / KOH / ethanol; H₂O / 36 h / Ambient temperature

With potassium hydroxide; potassium carbonate; In ethanol; water; acetone;
DOI:10.1080/00304949609356517