C₂₈H₃₃NO₆

Base Information

Chemical Name:C₂₈H₃₃NO₆
CAS No.:1402573-64-1
Molecular Formula:C₂₈H₃₃NO₆
Molecular Weight:479.573
Hs Code.:

C<sub>28</sub>H<sub>33</sub>NO<sub>6</sub>

Synonyms:C₂₈H₃₃NO₆

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Chemical Property of C₂₈H₃₃NO₆

Chemical Property:

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Technology Process of C₂₈H₃₃NO₆

There total 11 articles about C₂₈H₃₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₂₈H₃₃NO₆

: 1402573-64-1
C₂₈H₃₃NO₆

Guidance literature:: With sodium ethanolate; In ethanol; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1002/anie.201203379

Reference yield:

: 1402573-63-0
C₂₁H₂₇NO₄

: 94839-07-3
3,4-(methylenedioxy)-benzeneboronic acid

: 1402573-65-2
C₂₈H₃₃NO₆

: 1402573-64-1
C₂₈H₃₃NO₆

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine; In 1,4-dioxane; water; at 20 ℃; for 20h; optical yield given as %de;
DOI:10.1002/anie.201203379

Reference yield:

: C₁₉H₂₄N₂O₃

: 1402573-65-2
C₂₈H₃₃NO₆

: 1402573-64-1
C₂₈H₃₃NO₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / 1,4-dioxane / 48 h / 0 °C / Inert atmosphere

2.1: water / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: N,N’-bistosylhydrazine / toluene / 5 h / 100 °C / Inert atmosphere

4.2: 12 h / 20 °C / Inert atmosphere

5.1: silver trifluoromethanesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine / 1,4-dioxane; water / 20 h / 20 °C

With hydrogenchloride; chloro(1,5-cyclooctadiene)rhodium(I) dimer; N,N’-bistosylhydrazine; water; silver trifluoromethanesulfonate; Dess-Martin periodane; triethylamine; In 1,4-dioxane; dichloromethane; water; toluene;
DOI:10.1002/anie.201203379