N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

Base Information

Chemical Name:N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine
CAS No.:1258682-51-7
Molecular Formula:C₅₃H₈₂N₂O₄
Molecular Weight:811.245
Hs Code.:

Synonyms:N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

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Chemical Property of N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

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Technology Process of N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

There total 3 articles about N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 496-72-0
4-methyl-1,2-diaminobenzene

: 52123-16-7
4-hexadecyloxy-2-hydroxybenzaldehyde

: 1258682-51-7
N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

Guidance literature:: With acetic acid; In ethanol; for 3h; Reflux;
DOI:10.1016/j.poly.2010.08.017

Reference yield:

: 112-82-3
hexadecanyl bromide

: 1258682-51-7
N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogencarbonate; potassium iodide / acetone / 24 h / Reflux

2: acetic acid / ethanol / 4 h / Heating

With potassium hydrogencarbonate; acetic acid; potassium iodide; In ethanol; acetone;
DOI:10.1016/j.poly.2011.12.001

Reference yield:

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1258682-51-7
N,N'-bis(4-(4'-n-hexadecyloxy)salicylidene)-4-methyl-1,2-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogencarbonate; potassium iodide / acetone / 24 h / Reflux

2: acetic acid / ethanol / 4 h / Heating

With potassium hydrogencarbonate; acetic acid; potassium iodide; In ethanol; acetone;
DOI:10.1016/j.poly.2011.12.001