Technology Process of C24H39N3O16
There total 8 articles about C24H39N3O16 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; sodium methylate;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: copper(II) bis(trifluoromethanesulfonate) / dichloromethane / 20 °C / Inert atmosphere
3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / -20 °C / Molecular sieves acid washed
4.1: sodium methylate; methanol / 0.33 h / 20 °C / Inert atmosphere
With
methanol; trimethylsilyl trifluoromethanesulfonate; sodium methylate; acetic acid;
copper(II) bis(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine / 5 h / 0 - 20 °C
2.1: pyridine
3.1: acetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: copper(II) bis(trifluoromethanesulfonate) / dichloromethane / 20 °C / Inert atmosphere
5.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / -20 °C / Molecular sieves acid washed
6.1: sodium methylate; methanol / 0.33 h / 20 °C / Inert atmosphere
With
pyridine; methanol; trimethylsilyl trifluoromethanesulfonate; sodium methylate; acetic acid;
copper(II) bis(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane;