ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Base Information

Chemical Name:ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside
CAS No.:1309779-28-9
Molecular Formula:C₂₃H₃₈O₅SSi
Molecular Weight:454.703
Hs Code.:

Synonyms:ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Suppliers and Price of ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

There total 5 articles about ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 132799-09-8
ethyl 2-O-acetyl-4-O-benzyl-α-L-thiorhamnopyranoside

: 1309779-28-9
ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.201006327

Reference yield:

: 162466-37-7
C₁₈H₂₆O₅S

: 1309779-28-9
ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 0.08 h

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; acetic acid; In dichloromethane;
DOI:10.1002/anie.201006327

Reference yield:

: 100-39-0
benzyl bromide

: 1309779-28-9
ethyl 2-O-acetyl-3-O-triethylsilyl-4-O-benzyl-α-L-thiorhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil / Inert atmosphere

1.2: 17.5 h

2.1: acetic acid / 0.08 h

3.1: pyridine / dichloromethane / 0 - 20 °C

With pyridine; sodium hydride; acetic acid; In dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1002/anie.201006327