C₁₇H₂₅NO₃Si

Base Information

• Chemical Name: C₁₇H₂₅NO₃Si
• CAS No.: 1401229-71-7
• Molecular Formula: C₁₇H₂₅NO₃Si
• Molecular Weight: 319.476
• Mol file: 1401229-71-7.mol

Synonyms:C₁₇H₂₅NO₃Si

Chemical Property of C₁₇H₂₅NO₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₅NO₃Si

There total 4 articles about C₁₇H₂₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H31NO5Si → C17H25NO3Si (1401229-71-7)

Guidance literature:

With palladium on activated charcoal; hydrogen; In ethanol; at 20 ℃; for 3h;

DOI:10.1021/ol3024506

Reference yield:

tyrosine (556-02-5,18875-48-4,25619-78-7,30704-25-7) → C17H25NO3Si (1401229-71-7)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium hydroxide / water; 1,4-dioxane / 23 h / 0 - 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 30 h / 0 - 20 °C

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / 1,2-dichloro-ethane / 6 h / 0 - 20 °C

3.2: 3 h / Reflux

4.1: hydrogen; palladium on activated charcoal / ethanol / 3 h / 20 °C

With 1H-imidazole; dmap; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In 1,4-dioxane; ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1021/ol3024506

Reference yield:

N-α-benzyloxycarbonyl-D-tyrosine (64205-12-5) → C17H25NO3Si (1401229-71-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 30 h / 0 - 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / 1,2-dichloro-ethane / 6 h / 0 - 20 °C

2.2: 3 h / Reflux

3.1: hydrogen; palladium on activated charcoal / ethanol / 3 h / 20 °C

With 1H-imidazole; dmap; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1021/ol3024506

upstream raw materials:

tyrosine

N-α-benzyloxycarbonyl-D-tyrosine

C₂₃H₃₁NO₅Si

Downstream raw materials:

C₂₉H₄₅NO₄Si