methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside

Base Information

• Chemical Name: methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside
• CAS No.: 148693-27-0
• Molecular Formula: C₁₉H₁₉IO₄
• Molecular Weight: 438.262

Synonyms:methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside

Chemical Property of methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside

There total 1 articles about methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 2-Deoxy-3-O-(methylsulfonyl)-5-O-(4-phenylbenzoyl)-α-D-erythro-pentofuranoside (125611-96-3) + methyl iodide (74-88-4) → methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside (148693-27-0) + methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-erythro-pentafuranoside

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; Yield given. Multistep reaction. Yields of byproduct given; 1) toluene, -10 deg C, 0.5 h, 2) 80 deg C, 1.5 to 3 h;

DOI:10.1007/BF00808508

Reference yield: 74.0%

methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside (148693-27-0) → methyl 3-azido-2,3-dideoxy-5-O-(4-phenylbenzoyl)-α-D-erythro-pentofuranoside (149437-42-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 75 - 80 ℃;

DOI:10.1007/BF00808509

Reference yield: 71.0%

sodium thiobenzoate (51066-54-7) + methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside (148693-27-0) → methyl 3-benzoylthio-2,3-dideoxy-5-O-(4-phenylbenzoyl)-α-D-erythro-pentafuranoside (148693-31-6)

Guidance literature:

In N,N-dimethyl-formamide; at 75 ℃; for 3.5h;

DOI:10.1007/BF00808508

upstream raw materials:

Methyl 2-Deoxy-3-O-(methylsulfonyl)-5-O-(4-phenylbenzoyl)-α-D-erythro-pentofuranoside

methyl iodide

Downstream raw materials:

methyl 3-benzoylthio-2,3-dideoxy-5-O-(4-phenylbenzoyl)-α-D-erythro-pentafuranoside

methyl 3-azido-2,3-dideoxy-5-O-(4-phenylbenzoyl)-α-D-erythro-pentofuranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 148693-27-0 methyl 2,3-dideoxy-3-iodo-5-O-(4-phenylbenzoyl)-α-D-threo-pentofuranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send