(4Z)-8-(benzyloxy)-4-octenoyl chloride

Base Information

Chemical Name:(4Z)-8-(benzyloxy)-4-octenoyl chloride
CAS No.:763110-41-4
Molecular Formula:C₁₅H₁₉ClO₂
Molecular Weight:266.768
Hs Code.:

Synonyms:(4Z)-8-(benzyloxy)-4-octenoyl chloride

Suppliers and Price of (4Z)-8-(benzyloxy)-4-octenoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4Z)-8-(benzyloxy)-4-octenoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4Z)-8-(benzyloxy)-4-octenoyl chloride

There total 5 articles about (4Z)-8-(benzyloxy)-4-octenoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 763110-41-4
(4Z)-8-(benzyloxy)-4-octenoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.33 h / 0 °C

1.2: 65 percent / tetrahydrofuran / 1.5 h / -78 °C

2.1: 97 percent / aq. NaOH / tetrahydrofuran / 20 °C

3.1: oxalyl chloride / 3 h / 20 °C

With sodium hydroxide; oxalyl dichloride; sodium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1039/b406280a

Reference yield:

: 4541-14-4
4-benzyloxy-butan-1-ol

: 763110-41-4
(4Z)-8-(benzyloxy)-4-octenoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: 99 percent / DMSO; oxalyl chloride; Et₃N / CH₂Cl₂ / 2 h / -78 °C

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.33 h / 0 °C

2.2: 65 percent / tetrahydrofuran / 1.5 h / -78 °C

3.1: 97 percent / aq. NaOH / tetrahydrofuran / 20 °C

4.1: oxalyl chloride / 3 h / 20 °C

With sodium hydroxide; oxalyl dichloride; sodium hexamethyldisilazane; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 1.1: Swern oxidation;
DOI:10.1039/b406280a