[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

Base Information

Chemical Name:[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)
CAS No.:1350372-41-6
Molecular Formula:C₅₉H₅₂CuN₄O₂
Molecular Weight:912.633
Hs Code.:

Synonyms:[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

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Chemical Property of [5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

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Technology Process of [5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

There total 4 articles about [5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrin

: 1350372-41-6
[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

Guidance literature:: With copper diacetate; In methanol; chloroform; at 20 ℃; for 5h;
DOI:10.1039/c1ob06281f

Reference yield: 98.0%

: (2,4,6-Me₃C₆H₂)3((MeO)2C₁₀H₅)C₂₀H₁₀N₄

: 142-71-2
copper diacetate

: 1350372-41-6
[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

Guidance literature:: In dichloromethane; reaction of copper compd. with porphyrin deriv. in CH2Cl2 at room temp. for 5 h;
DOI:10.1039/c1ob06281f

Reference yield:

: 487-68-3
mesytaldehyde

: 1350372-41-6
[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-trimesitylporphyrinato]copper(II)

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / chloroform / 1.5 h / 20 °C

1.2: 0.25 h

2.1: copper diacetate / methanol; chloroform / 5 h / 20 °C

With boron trifluoride diethyl etherate; copper diacetate; In methanol; chloroform;
DOI:10.1039/c1ob06281f