benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

Base Information

Chemical Name:benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate
CAS No.:1052715-51-1
Molecular Formula:C₁₄H₁₆N₂O₄
Molecular Weight:276.292
Hs Code.:

Synonyms:benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

Chemical Property:

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Technology Process of benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

There total 7 articles about benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1052715-50-0
C₁₉H₂₈N₂O₇S

: 1052715-51-1
benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

Guidance literature:: With pyridine; at 120 ℃; for 2h;

Reference yield:

: 1312789-31-3,167832-26-0,1932598-12-3
(+/-)-benzyl 3-amino-4-hydroxypiperidine-1-carboxylate

: 1052715-51-1
benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 2 h / 20 - 30 °C

2: triethylamine / dichloromethane / 18 h / 20 - 30 °C

3: pyridine / 2 h / 120 °C

With pyridine; triethylamine; In dichloromethane;

Reference yield:

: 1052715-77-1,859854-67-4,1549812-60-3
benzyl (3S,4S)-3,4-trans-3-[(tert-butoxycarbonyl)amino]-4-hydroxypiperidine-1-carboxylate

: 1052715-51-1
benzyl (3aS,7aR)-2-oxohexahydro[1,3]oxazolo[4,5-c]pyridine-5(4H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 18 h / 20 - 30 °C

2: pyridine / 2 h / 120 °C

With pyridine; triethylamine; In dichloromethane;