(2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

Base Information

Chemical Name:(2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine
CAS No.:115018-45-6
Molecular Formula:C₅₉H₈₉NO₆Si
Molecular Weight:936.444
Hs Code.:

Synonyms:(2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

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Chemical Property of (2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

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Technology Process of (2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

There total 6 articles about (2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 115018-44-5
(2S,3R,4E,8E,2'R)-2-(2'-acetoxyhexadecanoyl)amino-1-O-benzoyl-4,8-octadiene-1,3-diol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 115018-45-6
(2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 70 ℃; for 5h;

Reference yield:

: 78715-84-1
4-formyl-2-phenyl-Δ²-oxazoline

: 115018-45-6
(2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

Guidance literature:: Multi-step reaction with 4 steps

1: hexane; diethyl ether; toluene / 1.5 h / Ambient temperature

2: 2 N HCl / H₂O; tetrahydrofuran / 21 h / Ambient temperature

3: 64 percent / pyridine / 19 h / 50 °C

4: 99 percent / imidazole / dimethylformamide / 5 h / 70 °C

With 1H-imidazole; hydrogenchloride; In tetrahydrofuran; pyridine; diethyl ether; hexane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 88195-82-8
p-nitrophenyl 2-O-acetyl-(2R)-2-hydroxypalmitate

: 115018-45-6
(2S,3R,4E,8E,2'R)-N-(2'-Acetoxyhexadecanoyl)-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-4,8-sphingadienine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / pyridine / 19 h / 50 °C

2: 99 percent / imidazole / dimethylformamide / 5 h / 70 °C

With 1H-imidazole; In pyridine; N,N-dimethyl-formamide;