4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol

Base Information

• Chemical Name: 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol
• CAS No.: 321883-86-7
• Molecular Formula: C₂₇H₂₈O₆
• Molecular Weight: 448.516

Synonyms:4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol

Chemical Property of 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol

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Technology Process of 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol

There total 1 articles about 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(4-vinylphenyl)magnesium bromide (18120-63-3) + sym-(keto)dibenzo-16-crown-5 (81633-82-1) → 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7(12),8,10,20,22-hexaen-4-ol (321883-86-7)

Guidance literature:

In tetrahydrofuran; for 6h; Heating;

DOI:10.1002/jhet.5570370554

Reference yield: 90.0%

bromoacetic acid (79-08-3) + 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7(12),8,10,20,22-hexaen-4-ol (321883-86-7) → [4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(20),7(12),8,10,21,23-hexaen-4-yloxy]-acetic acid

Guidance literature:

4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.0^7,12]tetracosa-1⁽²⁴⁾,7⁽¹²⁾,8,10,20,22-hexaen-4-ol; With potassium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

bromoacetic acid; In tetrahydrofuran; at 20 ℃;

DOI:10.1002/jhet.5570380201

Reference yield: 72.0%

ethyl bromoacetate (105-36-2) + 4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7(12),8,10,20,22-hexaen-4-ol (321883-86-7) → [4-(4-vinyl-phenyl)-2,6,13,16,19-pentaoxa-tricyclo[18.4.0.07,12]tetracosa-1(24),7,9,11,20,22-hexaen-4-yloxy]-acetic acid ethyl ester

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 ℃;

DOI:10.1002/jhet.5570410503

upstream raw materials:

(4-vinylphenyl)magnesium bromide

sym-(keto)dibenzo-16-crown-5

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