O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

Base Information

Chemical Name:O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate
CAS No.:108795-57-9
Molecular Formula:C₁₃H₁₄F₃N₃O₄S
Molecular Weight:365.333
Hs Code.:

Synonyms:O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

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Chemical Property of O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

Chemical Property:

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Technology Process of O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

There total 3 articles about O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108773-05-3
2-(2-hydroxy-3-nitrophenyl)-N-(trifluoroacetyl)ethylamine

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: 108795-57-9
O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at -5 ℃; for 0.75h;
DOI:10.1021/jm00390a009

Reference yield:

: 108773-31-5
2,2,2-trifluoro-N-(2-hydroxyphenethyl)acetamide

: 108795-57-9
O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / NaNO₃, La(NO₃)3*6H₂O, 6 N HCl / diethyl ether / 18 h / Ambient temperature

2: 93 percent / 0.5 N NaOH / tetrahydrofuran / 0.75 h / -5 °C

With hydrogenchloride; sodium hydroxide; sodium nitrate; lanthanum(III) nitrate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00390a009

Reference yield:

: 13062-80-1
2-(2-hydroxyphenyl)ethylamine hydrobromide

: 108795-57-9
O-<2-nitro-6-<2-(trifluoroacetamido)ethyl>phenyl>-N,N-dimethylthiocarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / diethyl ether / 1 h / Ambient temperature

2: 30 percent / NaNO₃, La(NO₃)3*6H₂O, 6 N HCl / diethyl ether / 18 h / Ambient temperature

3: 93 percent / 0.5 N NaOH / tetrahydrofuran / 0.75 h / -5 °C

With hydrogenchloride; sodium hydroxide; sodium nitrate; lanthanum(III) nitrate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00390a009