N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

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Chemical Name:N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine
CAS No.:1470268-11-1
Molecular Formula:C₄₆H₆₀BN₃O₄S
Molecular Weight:761.877
Hs Code.:

Synonyms:N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

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Chemical Property of N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

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Technology Process of N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

There total 3 articles about N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.9%

: 4,4,4',4',5,5,5'-heptamethyl-2,2'-bi(1,3,2-dioxaborolane)

: 1384289-48-8
N,N-di(4-octyloxyphenyl)-4-(7-(quinolin-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

: 1470268-11-1
N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In tetrahydrofuran; at 60 ℃; for 12h;
DOI:10.1016/j.dyepig.2014.03.040

Reference yield:

: 1384270-52-3
4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

: 1470268-11-1
N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; methanol / 12 h / 80 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / tetrahydrofuran / 12 h / 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In tetrahydrofuran; methanol; toluene;
DOI:10.1016/j.dyepig.2014.03.040

Reference yield:

: 15155-41-6
4,7-dibromobenzo[c][1,2,5]thiadiazole

: 1470268-11-1
N,N-di(4-octyloxyphenyl)-4-(7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; methanol / 12 h / 80 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / tetrahydrofuran / 12 h / 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In tetrahydrofuran; methanol; toluene;
DOI:10.1016/j.dyepig.2014.03.040