3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Base Information

Chemical Name:3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide
CAS No.:1169569-99-6
Molecular Formula:C₄₃H₆₁NO₆
Molecular Weight:687.96
Hs Code.:

Synonyms:3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Suppliers and Price of 3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

There total 8 articles about 3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 17347-61-4
2,2-dimethylsuccinic anhydride

: 1169569-24-7
3β-hydroxy-21-oxolup-18-en-28-oic acid N-benzylamide

: 1169569-99-6
3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Guidance literature:: With pyridine; dmap; Reflux;

Reference yield:

: 473-98-3
betulin

: 1169569-99-6
3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Guidance literature:: Multi-step reaction with 9 steps

1: pyridine / dmap / 5 h / 20 °C

2: acetic anhydride; hydrogen bromide; acetic acid / toluene / 4 h / 90 °C

3: acetic anhydride; sodium acetate; acetic acid; sodium dichromate dihydrate / toluene / 60 °C

4: potassium hydroxide; ethanol / toluene / 1 h / 20 °C

5: trifluoroacetic acid; sodium periodate; water / ruthenium (IV) oxide monohydrate / ethyl acetate / 20 °C

6: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

7: triethylamine / dichloromethane / 20 °C

8: sodium hydroxide; water / 1,4-dioxane / 4 h / 50 °C

9: pyridine / dmap / Reflux

With pyridine; sodium periodate; oxalyl dichloride; sodium dichromate dihydrate; ethanol; water; hydrogen bromide; sodium acetate; acetic anhydride; acetic acid; triethylamine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; dmap; ruthenium (IV) oxide monohydrate; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; ethyl acetate; toluene;

Reference yield:

: 226384-14-1
(3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-3a-(hydroxymethyl)-1-isopropyl-5a,5b,8, 8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-9-yl acetate

: 1169569-99-6
3β-O-(3',3'-dimethylsuccinyl)-21-oxolup-18-en-28-oic acid N-benzylamide

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid; sodium periodate; water / ruthenium (IV) oxide monohydrate / ethyl acetate / 20 °C

2: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

3: triethylamine / dichloromethane / 20 °C

4: sodium hydroxide; water / 1,4-dioxane / 4 h / 50 °C

5: pyridine / dmap / Reflux

With pyridine; sodium periodate; oxalyl dichloride; water; triethylamine; trifluoroacetic acid; sodium hydroxide; dmap; ruthenium (IV) oxide monohydrate; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; ethyl acetate;