Technology Process of C19H15F6N3Si
There total 3 articles about C19H15F6N3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: acetic acid / 20 h / 20 °C / Inert atmosphere
2: acetic acid; N-Bromosuccinimide / 1 h / 20 °C
3: copper(I) bromide dimethylsulfide complex; palladium diacetate; triphenylphosphine; triethylamine / 22 h / 50 °C / Inert atmosphere
With
N-Bromosuccinimide; copper(I) bromide dimethylsulfide complex; palladium diacetate; acetic acid; triethylamine; triphenylphosphine;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid; N-Bromosuccinimide / 1 h / 20 °C
2: copper(I) bromide dimethylsulfide complex; palladium diacetate; triphenylphosphine; triethylamine / 22 h / 50 °C / Inert atmosphere
With
N-Bromosuccinimide; copper(I) bromide dimethylsulfide complex; palladium diacetate; acetic acid; triethylamine; triphenylphosphine;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert-butyl methyl ether / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
1.3: 2 h / 40 - 50 °C / Inert atmosphere
2.1: acetic acid; N-Bromosuccinimide / 1 h / 20 °C
3.1: copper(I) bromide dimethylsulfide complex; palladium diacetate; triphenylphosphine; triethylamine / 22 h / 50 °C / Inert atmosphere
With
N-Bromosuccinimide; copper(I) bromide dimethylsulfide complex; tert-butyl methyl ether; palladium diacetate; acetic acid; triethylamine; triphenylphosphine;