[W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

Base Information

Chemical Name:[W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4
CAS No.:910294-15-4
Molecular Formula:BF₄*C₃₆H₃₁O₂P₂W₂
Molecular Weight:1012.09
Hs Code.:

Synonyms:[W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

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Chemical Property of [W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

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Technology Process of [W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

There total 1 articles about [W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 910327-76-3,483306-17-8
W₂Cp₂(μ-PPh₂)₂(CO)₂

: 910294-15-4
[W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

Guidance literature:: In diethyl ether; dichloromethane; (N2); a soln. of W complex in CH2Cl2 stirred at room temp. with HBF4*O(C2H5)2 in Et2O for 4 h; evapd. (vac.), washed (petroleum ether, CH2Cl2/petroleum ether), dissolved in CH2Cl2, filtered, solvent-removed;
DOI:10.1021/ic060544n

Reference yield: 72.0%

: 910294-15-4
[W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

: 910327-76-3,483306-17-8
W₂Cp₂(μ-PPh₂)₂(CO)₂

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; (N2); stirred at 263 K for 1 min; evapd. (vac.), chromd. (alumina, at 285 K, CH2Cl2/petroleum ether), solvent-removed; elem. anal.;
DOI:10.1021/ic060544n