Dimesitylboron fluoride

Base Information

Chemical Name:Dimesitylboron fluoride
CAS No.:436-59-9
Molecular Formula:C18H22BF
Molecular Weight:268.182
Hs Code.:29319090
European Community (EC) Number:628-702-8
DSSTox Substance ID:DTXSID30392743
Nikkaji Number:J1.400.809H
Wikidata:Q82191129
Mol file:436-59-9.mol

Synonyms:Dimesitylboron fluoride;436-59-9;Dimesitylfluoroborane;fluorodimesitylborane;Fluoro-bis(2,4,6-trimethylphenyl)borane;fluorobis(2,4,6-trimethylphenyl)borane;Borane, fluorobis(2,4,6-trimethylphenyl)-;MFCD00012203;dimesityifluoroborane;dimesityl boron fluoride;Dimesitylboron fluoride, 90%;SCHEMBL357015;C18H22BF;DTXSID30392743;AKOS005255155;FS-4897;fluoro[bis(2,4,6-trimethylphenyl)]borane;Bis-(2,4,6-trimethyl-phenyl)-fluoroborane;CS-0181842;D3890;FT-0757347

Suppliers and Price of Dimesitylboron fluoride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Dimesitylboron fluoride
50mg
$ 45.00

TCI Chemical
Dimesitylfluoroborane >98.0%(HPLC)
25g
$ 551.00

TCI Chemical
Dimesitylfluoroborane >98.0%(HPLC)
1g
$ 51.00

TCI Chemical
Dimesitylfluoroborane >98.0%(HPLC)
5g
$ 156.00

Sigma-Aldrich
Dimesitylboron fluoride 90%
5g
$ 210.00

Sigma-Aldrich
Dimesitylboron fluoride 90%
1g
$ 66.00

Crysdot
Fluorodimesitylborane 97%
5g
$ 351.00

Chem-Impex
Dimesitylboronfluoride,98%(HPLC) 98%(HPLC)
1G
$ 44.80

Chem-Impex
Dimesitylboronfluoride,98%(HPLC) 98%(HPLC)
250MG
$ 22.40

Chem-Impex
Dimesitylboronfluoride,≥98%(HPLC)Hazmat ≥98%(HPLC)
5G
$ 157.25

Total 26 raw suppliers

Chemical Property of Dimesitylboron fluoride

Chemical Property:

Vapor Pressure:3.59E-05mmHg at 25°C
Melting Point:69-72 °C(lit.)
Refractive Index:1.518
Boiling Point:364.2 °C at 760 mmHg
Flash Point:174.1 °C
PSA：0.00000
Density:0.98 g/cm³
LogP:3.61220
Solubility.:soluble in Acetone,Ether
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:268.1798590
Heavy Atom Count:20
Complexity:265

Purity/Quality:

≥90% ^*data from raw suppliers

Dimesitylboron fluoride ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C
Statements: 34
Safety Statements: 26-27-28-36/37/39-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:B(C1=C(C=C(C=C1C)C)C)(C2=C(C=C(C=C2C)C)C)F

Technology Process of Dimesitylboron fluoride

There total 7 articles about Dimesitylboron fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 109-63-7
trifluoroborane diethyl ether

: 2633-66-1
2-mesitylmagnesium bromide

: MgBrF

: 436-59-9
dimesitylfluoroborane

Guidance literature:: In diethyl ether; addn. of MesMgBr in Et2O over a period of 1.5 h to BF3 in Et2O, refluxed for 3 h; removal of solvent in vac., sublimation (100°C, 1E-1 Torr);
DOI:10.1016/S0020-1693(00)83809-8

Reference yield: 81.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 109-63-7
boron trifluoride diethyl etherate

: 436-59-9
dimesitylfluoroborane

Guidance literature:: 2,4,6-trimethylphenyl bromide; With magnesium; In tetrahydrofuran; ethylene dibromide; for 3h; Reflux;

boron trifluoride diethyl etherate; In tetrahydrofuran; ethylene dibromide; at -20 ℃; Reflux;
DOI:10.1002/chem.202101687

Reference yield: 78.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 436-59-9
dimesitylfluoroborane

Guidance literature:: 2,4,6-trimethylphenyl bromide; With magnesium; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;

With boron trifluoride diethyl etherate; at 0 ℃; for 2h; Reflux;