C₄₉H₅₈N₄O₉Si

Base Information

Chemical Name:C₄₉H₅₈N₄O₉Si
CAS No.:1430098-18-2
Molecular Formula:C₄₉H₅₈N₄O₉Si
Molecular Weight:875.106
Hs Code.:

C<sub>49</sub>H<sub>58</sub>N<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₄₉H₅₈N₄O₉Si

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Chemical Property of C₄₉H₅₈N₄O₉Si

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Technology Process of C₄₉H₅₈N₄O₉Si

There total 14 articles about C₄₉H₅₈N₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430098-26-2
(2S, 3S)-3-O-(pyrrole-2-carbonyloxy)-2-N-Boc-allo-threonine

: C₃₅H₄₀N₂O₄Si

: 1430098-18-2
C₄₉H₅₈N₄O₉Si

Guidance literature:: (2S, 3S)-3-O-(pyrrole-2-carbonyloxy)-2-N-Boc-allo-threonine; With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h; Inert atmosphere;

C₃₅H₄₀N₂O₄Si; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.12.111

Reference yield:

: 742060-65-7
Boc-L-allo-Thr-OBn

: 1430098-18-2
C₄₉H₅₈N₄O₉Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 760.05 Torr / Inert atmosphere

3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2012.12.111

Reference yield:

: 634-97-9
pyrrole-2-carboxyl acid

: 1430098-18-2
C₄₉H₅₈N₄O₉Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 4 h / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 760.05 Torr / Inert atmosphere

4.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2012.12.111