(E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide

Base Information

• Chemical Name: (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide
• CAS No.: 1432726-62-9
• Molecular Formula: C₂₉H₄₀INO₃S
• Molecular Weight: 609.612

Synonyms:(E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide

Chemical Property of (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide

Chemical Property:

Purity/Quality:

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Technology Process of (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide

There total 3 articles about (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N-(2-iodo-4-methylphenyl)formamide (1304143-78-9) + 1-(para-toluenesulfonyl)tetradecyne (1432726-55-0) → (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide (1432726-62-9)

Guidance literature:

With potassium carbonate; In water; N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1002/chem.201202307

Reference yield:

p-tolyl benzeneselenosulfonate (68819-94-3) → (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide (1432726-62-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: chloroform / 2.5 h / Irradiation

1.2: 3.42 h / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide; water / 16 h / 20 °C

With potassium carbonate; In chloroform; water; N,N-dimethyl-formamide;

DOI:10.1002/chem.201202307

Reference yield:

1-tetradecyne (765-10-6) → (E)-N-(2-iodo-4-methylphenyl)-N-[(1-p-toluenesulfonyl)tetradec-2-en-2-yl]-formamide (1432726-62-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: chloroform / 2.5 h / Irradiation

1.2: 3.42 h / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide; water / 16 h / 20 °C

With potassium carbonate; In chloroform; water; N,N-dimethyl-formamide;

DOI:10.1002/chem.201202307

upstream raw materials:

N-(2-iodo-4-methylphenyl)formamide

1-(para-toluenesulfonyl)tetradecyne

p-tolyl benzeneselenosulfonate

1-tetradecyne

Downstream raw materials:

2-n-dodecyl-5-methyl-3-(p-toluenesulfonyl)-1H-indole

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