N₄-allyl-N₂-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N₄-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Base Information

• Chemical Name: N₄-allyl-N₂-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N₄-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine
• CAS No.: 1356010-49-5
• Molecular Formula: C₂₉H₃₁N₇O
• Molecular Weight: 493.611

Synonyms:N₄-allyl-N₂-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N₄-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Chemical Property of N₄-allyl-N₂-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N₄-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Chemical Property:

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Technology Process of N₄-allyl-N₂-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N₄-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

There total 12 articles about N₄-allyl-N₂-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N₄-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)aniline (1356009-07-8) + N-allyl-2-chloro-N-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-4-amine (1356009-68-1) → N4-allyl-N2-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N4-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine (1356010-49-5)

Guidance literature:

at 150 ℃; for 0.75h;

Reference yield:

cyclopentanone (120-92-3) → N4-allyl-N2-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N4-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine (1356010-49-5)

Guidance literature:

Multi-step reaction with 9 steps

1.1: diethyl ether; tetrahydrofuran / 2.5 h / 0 °C / Reflux

2.1: formic acid; dihydrogen peroxide / 4 h / 20 - 40 °C

3.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

3.2: 3 h / 25 °C

4.1: potassium hydroxide / water / 20 °C

5.1: hydrogenchloride; water / 1 h / Reflux

6.1: ammonia / water / 5 h / Heating

7.1: trichlorophosphate / 1 h / 110 °C / microwave irradiation

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 18 h / 20 °C

9.1: 0.75 h / 150 °C

With hydrogenchloride; n-butyllithium; formic acid; ammonia; water; dihydrogen peroxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; hexanes; diethyl ether; water; acetonitrile;

Reference yield:

phenylmagnesium bromide (100-58-3) → N4-allyl-N2-(3-(allyloxy)-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl)-N4-methyl-7-phenyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine (1356010-49-5)

Guidance literature:

Multi-step reaction with 9 steps

1.1: diethyl ether; tetrahydrofuran / 2.5 h / 0 °C / Reflux

2.1: formic acid; dihydrogen peroxide / 4 h / 20 - 40 °C

3.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

3.2: 3 h / 25 °C

4.1: potassium hydroxide / water / 20 °C

5.1: hydrogenchloride; water / 1 h / Reflux

6.1: ammonia / water / 5 h / Heating

7.1: trichlorophosphate / 1 h / 110 °C / microwave irradiation

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 18 h / 20 °C

9.1: 0.75 h / 150 °C

With hydrogenchloride; n-butyllithium; formic acid; ammonia; water; dihydrogen peroxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; hexanes; diethyl ether; water; acetonitrile;

upstream raw materials:

cyclopentanone

phenylmagnesium bromide

3,4-difluoronitrobenzene

cyclopent-1-en-1-ylbenzene

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