4-(diphenylphosphanyl)dibenzofurane

Base Information Edit

Chemical Name:4-(diphenylphosphanyl)dibenzofurane
CAS No.:133850-82-5
Molecular Formula:C₂₄H₁₇OP
Molecular Weight:352.372
Hs Code.:
Mol file:133850-82-5.mol

Synonyms:4-(diphenylphosphanyl)dibenzofurane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(diphenylphosphanyl)dibenzofurane Edit

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Technology Process of 4-(diphenylphosphanyl)dibenzofurane

There total 2 articles about 4-(diphenylphosphanyl)dibenzofurane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 132-64-9,214827-48-2
dibenzofuran

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 133850-82-5
4-(diphenylphosphanyl)dibenzofurane

Guidance literature:: dibenzofuran; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 - 20 ℃;

chloro-diphenylphosphine; In tetrahydrofuran; hexane; at -78 - 20 ℃; regioselective reaction;
DOI:10.1002/chem.201001981

Reference yield:

: 132-64-9,214827-48-2
dibenzofuran

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 133850-82-5
4-(diphenylphosphanyl)dibenzofurane

: 133850-81-4
4,6-bis(diphenylphosphanyl)dibenzofuran

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; Yield given. Multistep reaction. Yields of byproduct given; 1.a.) n-hexane, room temperature, b.) reflux, 1 h, 2.a.) n-hexane, 0 deg C, b.) 12 h, room temperature;