5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether

Base Information

Chemical Name:5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether
CAS No.:372075-92-8
Molecular Formula:C₂₁H₂₇BrN₄O₃
Molecular Weight:463.374
Hs Code.:

Synonyms:5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether

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Chemical Property of 5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether

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Technology Process of 5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether

There total 1 articles about 5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 111-24-0
1,5-dibromo-pentane

: 2872-52-8
disperse red 1

: 372075-92-8
5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether

Guidance literature:: disperse red 1; With potassium hydroxide; 18-crown-6 ether; In tetrahydrofuran; at 20 ℃; for 1h;

1,5-dibromo-pentane; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1002/ejoc.200801302

Reference yield: 89.0%

: 372075-92-8
5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether

: 105-53-3
diethyl malonate

: 1174752-21-6
diethyl 2-{5'-[2''-(N-ethyl-N-{4'''-[(4''''-nitrophenyl)azo]phenyl}amino)ethoxy]pentyl}malonate

Guidance literature:: 5-bromopentyl 2-(N-ethyl-N-{4'-[(4''-nitrophenyl)azo]phenyl}amino)ethyl ether; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

diethyl malonate; In tetrahydrofuran; for 20h; Reflux;
DOI:10.1002/ejoc.200801302