Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

Base Information

Chemical Name:Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester
CAS No.:137664-72-3
Molecular Formula:C₁₉H₂₈O₄
Molecular Weight:320.429
Hs Code.:

Synonyms:Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

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Chemical Property of Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

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Technology Process of Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

There total 3 articles about Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 137819-50-2
(3R,4R)-1-(benzyloxy)-4-methylhex-5-en-3-ol

: 137664-72-3
Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

Guidance literature:: With n-butyllithium;
DOI:10.1021/ja992134m

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 137664-72-3
Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi; t-BuOK; (-)-(Ipc)2BOMe

1.2: BF₃*Et₂O / tetrahydrofuran / -78 °C

1.3: H₂O₂; aq. NaOH / 40 °C

2.1: 90 percent / n-BuLi

With n-butyllithium; potassium tert-butylate; (-)-B-methoxydiisopinocampheylborane; 1.1: Addition / 1.2: allylboration / 1.3: Oxidation / 2.1: Substitution;
DOI:10.1021/ja992134m

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 137664-72-3
Carbonic acid (1R,2R)-1-(2-benzyloxy-ethyl)-2-methyl-but-3-enyl ester tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1) n-BuLi / 1) Et₂O, -78 deg C, 2) THF, 0 deg C

With n-butyllithium;
DOI:10.1016/S0040-4039(00)93479-8