C₄₇H₆₅IO₅

Base Information

Chemical Name:C₄₇H₆₅IO₅
CAS No.:1256563-90-2
Molecular Formula:C₄₇H₆₅IO₅
Molecular Weight:836.935
Hs Code.:

C<sub>47</sub>H<sub>65</sub>IO<sub>5</sub>

Synonyms:C₄₇H₆₅IO₅

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Chemical Property of C₄₇H₆₅IO₅

Chemical Property:

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Technology Process of C₄₇H₆₅IO₅

There total 8 articles about C₄₇H₆₅IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1256563-88-8
C₂₈H₃₇IO₂

: 2,5-bishexyloxy-4-vinylbenzaldehyde

: 1256563-90-2
C₄₇H₆₅IO₅

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In chloroform; for 40h; stereospecific reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol102398y

Reference yield:

: 111-25-1
1-bromo-hexane

: 1256563-90-2
C₄₇H₆₅IO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrosulfite pentahydrate; tetrabutylammomium bromide; potassium hydroxide / water; toluene / Cooling with ice; Reflux

2.1: Iodine monochloride / methanol / Cooling with ice; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform / 40 h / Inert atmosphere; Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; sodium hydrosulfite pentahydrate; potassium tert-butylate; tetrabutylammomium bromide; Iodine monochloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene; 4.1: Wittig reaction;
DOI:10.1021/ol102398y

Reference yield:

: 67399-93-3
1,4-dihexyloxybenzene

: 1256563-90-2
C₄₇H₆₅IO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: Iodine monochloride / methanol / Cooling with ice; Reflux

2.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform / 40 h / Inert atmosphere; Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; potassium tert-butylate; Iodine monochloride; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; 3.1: Wittig reaction;
DOI:10.1021/ol102398y