methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside
CAS No.:939051-51-1
Molecular Formula:C₆₀H₇₄O₁₅S
Molecular Weight:1067.3
Hs Code.:

methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Synonyms:methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

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Chemical Property of methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Chemical Property:

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Technology Process of methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

There total 13 articles about methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-D-arabino-hexopyranosyl) trichloroacetimidate

: 939051-48-6
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

: 939051-51-1
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

: methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-α-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: With triethylsilane; iodine; In toluene; at -94 ℃; for 4h;
DOI:10.1002/anie.200604031

Reference yield:

: 939050-75-6
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

: 939051-51-1
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NaNH₂ / dimethylformamide / 1 h / 70 °C / microwave irradiation

2: I₂; Et₃SiH / toluene / 2 h / -94 °C

3: 76 percent / NaNH₂ / dimethylformamide / 1 h / 70 °C / microwave irradiation

4: I₂; Et₃SiH / toluene / 4 h / -94 °C

With triethylsilane; iodine; sodium amide; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200604031

Reference yield:

: 939051-42-0
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

: 939051-51-1
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-(3-O-benzyl-4-O-benzylsulfonyl-2,6-dideoxy-β-D-arabinohexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaNH₂ / dimethylformamide / 1 h / 70 °C / microwave irradiation

2: I₂; Et₃SiH / toluene / 4 h / -94 °C

With triethylsilane; iodine; sodium amide; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200604031