N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

Base Information

Chemical Name:N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane
CAS No.:277760-02-8
Molecular Formula:C₄₁H₅₆N₄O₈S₄
Molecular Weight:861.182
Hs Code.:

N<sup>1</sup>,N<sup>5</sup>,N<sup>11</sup>,N<sup>15</sup>-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

Synonyms:N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

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Chemical Property of N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

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Technology Process of N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

There total 3 articles about N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 278807-16-2
C₂₉H₄₄N₄O₆S₂

: 277760-02-8
N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

Guidance literature:: C₂₉H₄₄N₄O₆S₂; With hydrogenchloride; at 70 ℃; for 1h;

p-toluenesulfonyl chloride; With triethylamine; In pyridine; at 20 ℃; for 4h;
DOI:10.1016/S0968-0896(00)00156-5

Reference yield:

: 67508-30-9
N¹,N⁵-di(p-toluenesulfonyl)-1,5-diaminopentane

: 277760-02-8
N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

Guidance literature:: Multi-step reaction with 3 steps

2.1: N₂H₄ / dimethylformamide / 24 h / 70 °C

3.1: 1.2 M HCl / 1 h / 70 °C

3.2: Et₃N / pyridine / 4 h / 20 °C

With hydrogenchloride; hydrazine; In N,N-dimethyl-formamide; 1.1: Alkylation / 2.1: Reduction / 3.1: decarbonylation / 3.2: Tosylation;
DOI:10.1016/S0968-0896(00)00156-5

Reference yield:

: 278807-15-1
C₄₃H₄₈N₄O₈S₂

: 277760-02-8
N¹,N⁵,N¹¹,N¹⁵-tetra(p-toluenesulfonyl)-1,15-diamino-5,11-diazapentadecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: N₂H₄ / dimethylformamide / 24 h / 70 °C

2.1: 1.2 M HCl / 1 h / 70 °C

2.2: Et₃N / pyridine / 4 h / 20 °C

With hydrogenchloride; hydrazine; In N,N-dimethyl-formamide; 1.1: Reduction / 2.1: decarbonylation / 2.2: Tosylation;
DOI:10.1016/S0968-0896(00)00156-5