N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

Base Information

Chemical Name:N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide
CAS No.:127826-99-7
Molecular Formula:C₁₈H₂₂N₂S₂
Molecular Weight:330.518
Hs Code.:

Synonyms:N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

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Technology Process of N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

There total 3 articles about N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 2801-21-0
benzothiazole sulfenamide

: 127826-98-6
(+/-)-(1,5,5-trimethyl-2-cyclohexen-1-yl)acetaldehyde

: 127826-99-7
N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

Guidance literature:: With sodium hydroxide; In ethanol; water; at 65 ℃; for 0.75h;
DOI:10.1016/S0040-4020(01)80849-8

Reference yield:

: 470-99-5
isophorol

: 127826-99-7
N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / mercuric acetate , allyl alcohol / 24 h / 33 °C

2: 75 percent / 0.5 h / 215 °C

3: 48 percent / 2 N sodium hydroxide / ethanol; H₂O / 0.75 h / 65 °C

With sodium hydroxide; mercury(II) diacetate; allyl alcohol; In ethanol; water;
DOI:10.1016/S0040-4020(01)80849-8

Reference yield:

: 124938-43-8
3-(ethenyloxy)-1,5,5-trimethylcyclohexene

: 127826-99-7
N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzothiazolesulfenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 0.5 h / 215 °C

2: 48 percent / 2 N sodium hydroxide / ethanol; H₂O / 0.75 h / 65 °C

With sodium hydroxide; In ethanol; water;
DOI:10.1016/S0040-4020(01)80849-8