Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

Base Information

Chemical Name:Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester
CAS No.:84325-60-0
Molecular Formula:C₂₇H₂₁ClN₂O₄S
Molecular Weight:504.994
Hs Code.:

Synonyms:Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

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Chemical Property of Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

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Technology Process of Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

There total 6 articles about Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-24-7
acetic anhydride

: 84325-51-9
10-chloro-6-(4-methoxyanilino)-5H-benzo[a]-phenothiazin-5-one

: 84325-60-0
Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

Guidance literature:: With zinc; In pyridine; 1) 20 min, room temperature, 2) 45 min, reflux;

Reference yield:

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 84325-60-0
Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2-picoline / various solvent(s) / 4 h / Heating

2: 79 percent / pyridine / 3 h / Heating

3: 87 percent / zinc dust / pyridine / 1) 20 min, room temperature, 2) 45 min, reflux

With α-picoline; zinc; In pyridine;

Reference yield:

: 22359-32-6
2-chloro-3-(4-methoxyphenyl)amino-1,4-naphthoquinone

: 84325-60-0
Acetic acid 12-acetyl-10-chloro-6-(4-methoxy-phenylamino)-12H-benzo[a]phenothiazin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / 3 h / Heating

2: 87 percent / zinc dust / pyridine / 1) 20 min, room temperature, 2) 45 min, reflux

With zinc; In pyridine;