N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

Base Information

Chemical Name:N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide
CAS No.:175354-29-7
Molecular Formula:C₁₅H₂₆N₂O₅
Molecular Weight:314.382
Hs Code.:

Synonyms:N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

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Chemical Property of N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

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Technology Process of N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

There total 3 articles about N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 56074-21-6
N-((tert-butyloxy)carbonyl)iminodiacetic acid anhydride

: 175354-29-7
N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

Guidance literature:: In N,N-dimethyl-formamide; for 20h;
DOI:10.1016/j.bmc.2004.04.031

Reference yield:

: 56074-20-5
N-((tert-butyloxy)carbonyl)iminodiacetic acid

: 108-91-8,157973-60-9
cyclohexylamine

: 175354-29-7
N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Yield given. Multistep reaction; 1.) DMF, 25 deg C, 1 h, 2.) DMF, 25 deg C, 20 h;
DOI:10.1021/ja9530681

Reference yield:

: 56074-20-5
N-((tert-butyloxy)carbonyl)iminodiacetic acid

: 175354-29-7
N-((tert-butyloxy)carbonyl)-N'-cyclohexyliminodiacetic acid monoamide

Guidance literature:: Multi-step reaction with 2 steps

1: EDCI / dimethylformamide / 1 h / 20 °C

2: 0.3 g / dimethylformamide / 20 h

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.04.031