{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

Base Information

Chemical Name:{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol
CAS No.:1018479-95-2
Molecular Formula:C₃₀H₅₂O₅Si
Molecular Weight:520.825
Hs Code.:

{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

Synonyms:{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

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Chemical Property of {(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

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Technology Process of {(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

There total 1 articles about {(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1018479-86-1
(1S,8R,4aR)-1-[(4-methoxyphenyl)methoxy]-8,4a-dimethyl-4,7-dimethylene-8-[2-(tert-butyldimethylsilanyloxy)ethyl]-1,2,3,5,6,8,4a,8a-octahydronaphthalene

: 1018479-95-2
{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

Guidance literature:: (1S,8R,4aR)-1-[(4-methoxyphenyl)methoxy]-8,4a-dimethyl-4,7-dimethylene-8-[2-(tert-butyldimethylsilanyloxy)ethyl]-1,2,3,5,6,8,4a,8a-octahydronaphthalene; With borane-THF; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; for 6h; Inert atmosphere;
DOI:10.1021/ol800101v

Reference yield:

: 1018479-95-2
{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

: 1018479-96-3
(4S,5R,8aR)-4-[(4-methoxyphenyl)methoxy]-5,8a-dimethyl-5-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphthalene-1,6-dicarbaldehyde

Guidance literature:: With dipyridinium dichromate; sodium acetate; In dichloromethane; at 20 ℃; for 2h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol800101v

Reference yield:

: 1018479-95-2
{(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol

: 1018479-87-2
(4S,1R,5R,6R,8aR)-4-[(4-methoxyphenyl)methoxy]-5,8a-dimethyl-5-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphthalene-1,6-dicarbaldehyde

Guidance literature:: {(1S,8S,4aS)-5-(hydroxymethyl)-8-[(4-methoxyphenyl)methoxy]-1,4a-dimethyl-1-[2-(tert-butyldimethylsilanyloxy)ethyl]perhydronaphth-2-yl}methan-1-ol; With dipyridinium dichromate; sodium acetate; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere; Molecular sieve;

With sodium methylate; In methanol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol800101v