(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

Base Information

Chemical Name:(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol
CAS No.:1240304-62-4
Molecular Formula:C₃₂H₃₉BrO₁₀
Molecular Weight:663.56
Hs Code.:

Synonyms:(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

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Chemical Property of (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

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Technology Process of (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

There total 25 articles about (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1240304-73-7
C₂₄H₃₁BrO₇

: 108-24-7
acetic anhydride

: 1240304-62-4
(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

Guidance literature:: C₂₄H₃₁BrO₇; acetic anhydride; With pyridine; at 20 ℃; for 15h;

With triethylsilane; boron trifluoride diethyl etherate; In chloroform; acetonitrile; at 4 ℃; for 0.5h; Inert atmosphere;

Reference yield: 46.0%

: (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-hydroxy-4-(propan-2-yl)phenyl}-D-glucitol

: 74-88-4
methyl iodide

: 1240304-62-4
(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 50 ℃;

Reference yield:

: C₃₂H₃₉BrO₁₁

: 1240304-62-4
(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromo-2-methylphenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In chloroform; acetonitrile; at 4 ℃; for 0.5h; Inert atmosphere;