4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside)

Base Information

• Chemical Name: 4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside)
• CAS No.: 1133352-64-3
• Molecular Formula: C₅₃H₆₂O₁₂Si₂
• Molecular Weight: 947.239

Synonyms:4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside)

Chemical Property of 4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside)

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Technology Process of 4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside)

There total 1 articles about 4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

1-(4-(tert-butyldimethylsilyloxy)-2,6-dihydroxyphenyl)-3-(4-(tert-butyldimethylsilyloxy)phenyl)propan-1-one (1133352-60-9) + 2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide (22860-91-9) → 4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside) (1133352-64-3)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 ℃; for 18h; Molecular sieve;

DOI:10.1016/j.bmcl.2008.11.112

Reference yield: 27.0%

4'-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy)phenyl)-2',6'-dihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside) (1133352-64-3) → 3-(4-hydroxyphenyl)-2',4',6'-trihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside) (1133352-66-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1016/j.bmcl.2008.11.112

upstream raw materials:

1-(4-(tert-butyldimethylsilyloxy)-2,6-dihydroxyphenyl)-3-(4-(tert-butyldimethylsilyloxy)phenyl)propan-1-one

2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide

Downstream raw materials:

3-(4-hydroxyphenyl)-2',4',6'-trihydroxypropiophenone 2'-O-(2'',3'',5''-tribenzoyl-β-D-ribofuranoside)

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